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Séparation chromatographique sur papier et dosage des anions à l'échelle du microgramme - Silicium, Bore, Molybdène

par Lacourt, Alice ;Sommereyns, Ghislaine ;Claret, Michel
Référence Mikrochimica acta, 38, 4, page (444-455)
Publication Publié, 1951-12

Article révisé par les pairs

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Résumé :

Microgram paper chromatography has succeeded to separate Silicate, Borate and Molybdate of Sodium. Development takes only 60′ using acetone, HCl 5% (acetone containing 5 ml of concentrated HCl in ml) in a vessel saturated with 2-Butanone, HCl 5%. The procedure has been checked quantitatively with mixtures containing 10 micrograms of each element. Boron has been determined absorptiometrically after development and elution. It is recovered to ± 3%. © 1951 Springer-Verlag.